[PDF] Batch Processing: Modeling and Design By Urmila Diwekar Book Free Download

Download Batch Processing: Modeling and Design By Urmila Diwekar – Although batch processing has existed for a long time, designing these processes and unit operations has been considered an onerous task that required computational efforts. Design of these processes is made more complex because of the time dependent nature of the process and the allowable flexibility. More often than not, every unit encounters optimal control problems. Therefore, traditional design books have not covered batch processing in detail. Filling this void, Batch Processing: Modeling and Design describes various unit operations in batch and bio-processing as well as design methods for these units.

Topics include:

• Batch distillation operating modes and configurations
• Batch absorption operations based on the solubility difference
• Batch adsorption based on differential affinity of various soluble molecules to solid absorbents
• Batch chromatography for measuring a wide variety of thermodynamic, kinetic, and physico-chemical properties
• Batch crystallization where a phase is used to find the supersaturation at which point material crystallizes
• Batch drying that stresses the phase diagram of water to describe this operation
• Batch filtration using a porous medium or screen to separate solids from liquids
• Batch centrifugation where centrifugal force is used for separation

Batch processes are widely used in pharmaceutical, food, and specialty chemicals where high value, low volume products are manufactured. Recent developments in bio-based manufacturing also favor batch processes because feed variations can be easily handled in batch processes. Further, the emerging area of nanomaterials manufacturing currently uses batch processes as they are low volume, high energy intensive processes. With examples, case studies, and more than 100 homework problems, this book describes the unit operations in batch and bioprocessing and gives students a thorough grounding in the numerical methods necessary to solve these design problems.

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Book Contents

• Introduction
  Batch Separation
  Optimization and Optimal Control
  Summary
  Numerical Methods for Integration
  Error and Stability
  Numerical Integration Techniques
  Orthogonal Collocation Method
  Summary
• Batch Reactors
  Classification of Reactions and Reaction Kinetics
  Irreversible Reactions
  Reversible Reactions
  Reactions in Parallel
  Reactions in Series
  Autocatalytic Reactions
  Biodiesel Production: A Case Study
  Summary
• Batch Distillation
  Early Theoretical Analysis
  Hierarchy of Models
  Shortcut Model
  Optimization and Optimal Control
  Complex Systems
  Computer Aided Design Software
  Summary
• Optimization and Optimal Control
  Optimization Problems and Software
  Convex and Concave Functions
  Linear Programming
  Nonlinear Programming
  Discrete Optimization
  Optimal Control
  Summary
• Batch Absorption
  Absorption Dynamics
  Summary
• Batch Extraction
  Solid Extraction or Leaching
  Rate of Extraction
  Liquid-Liquid Extraction
  Summary
• Batch Adsorption
  Adsorption Equilibrium
  Fixed Bed or Packed Bed Adsorption
  Summary
• Batch Chromatography
  Retention Theory
  Plate Model
  Resolution
  Summary
• Batch Crystallization
  Phase Diagram
  Supersaturation
  Crystallization Kinetics
  Modeling Cooling Batch Crystallization
  Modeling Evaporative Batch Crystallization
  Optimal Control Problems
  Summary
• Batch Drying
  Thermodynamics of Drying
  Rate of Drying
  Types of Dryers
  Summary
• Batch Filtration
  Conventional or Dead-End Filtration
  Crossflow Filtration
  Types of Filtration Equipment
  Summary
  Batch Centrifugation
  Sedimentation in a Centrifugal Field
  Filtration in Centrifugal Field
  Summary
• Batch Scheduling and Planning
  Types of Scheduling Problems
  Role of Optimization in Batch Scheduling
  Industrial Scheduling Problem
  Summary
• Batch Process Simulation
  Introduction
  Detailed Modeling of Single Batch Processes
  Modeling of Multiproduct Batch Plants
  Summary

About Author

Urmila Diwekar

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